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International Starch Institute
Science Park Aarhus, Denmark
ISI 06 Table 1c - Determination of Dry Matter in
Acid Converted 55 DE Syrup by Refractive Index
| 1. Scope | The table is applicable to 55 DE acid converted syrup with 0.4% ash on dry matter. | LT 24 Nov. 1997 | ||||
| 2. Principle | The refractive index of sample is transformed to dry matter by a table. | |||||
| 3. Apparatus | 3.1 Refractometer with thermostat | |||||
| 4. Procedure | Adjust temperature of refractometer (3.1) to 20, 30, 45 or 60 oC. | +/- 0.2 oC | ||||
| Adjust sample temperature to that chosen for the refractometer. | ||||||
| Place a few drops of sample on fixed prism and close instrument | Work fast | |||||
| Read the refractive index (nD) to nearest 0.0002 unit. | Clean prisms immediately after. | |||||
| 5. Calculation | Find dry matter (DM) in percent of sample (average results of two samples with no decimal) by using table: | Correct eventually for differing DE | ||||
DM% |
20 oC |
30 oC |
45 oC |
60 oC |
||
0 |
1,33299 |
1,33194 |
1,32985 |
1,32725 |
||
2 |
1,33590 |
1,33483 |
1,33271 |
1,33008 |
||
4 |
1,33890 |
1,33780 |
1,33564 |
1,33299 |
||
6 |
1,34195 |
1,34081 |
1,33863 |
1,33595 |
||
8 |
1,34504 |
1,34388 |
1,34166 |
1,33896 |
||
10 |
1,34818 |
1,34699 |
1,34474 |
1,34202 |
||
12 |
1,35137 |
1,35016 |
1,34787 |
1,34513 |
||
14 |
1,35461 |
1,35337 |
1,35106 |
1,34828 |
||
16 |
1,35790 |
1,35663 |
1,35429 |
1,35149 |
||
18 |
1,36124 |
1,35995 |
1,35757 |
1,35476 |
||
20 |
1,36463 |
1,36331 |
1,36091 |
1,35807 |
||
22 |
1,36807 |
1,36673 |
1,36430 |
1,36144 |
||
24 |
1,37157 |
1,37020 |
1,36774 |
1,36486 |
||
26 |
1,37512 |
1,37373 |
1,37123 |
1,36834 |
||
28 |
1,37872 |
1,37731 |
1,37479 |
1,37187 |
||
30 |
1,38238 |
1,38094 |
1,37839 |
1,37546 |
||
32 |
1,38610 |
1,38463 |
1,38206 |
1,37910 |
||
34 |
1,38987 |
1,38838 |
1,38578 |
1,38281 |
||
36 |
1,39370 |
1,39218 |
1,38956 |
1,38657 |
||
38 |
1,39758 |
1,39605 |
1,39339 |
1,39039 |
||
40 |
1,40153 |
1,39997 |
1,39729 |
1,39427 |
||
42 |
1,40554 |
1,40395 |
1,40125 |
1,39822 |
||
44 |
1,40960 |
1,40800 |
1,40527 |
1,40222 |
||
46 |
1,41373 |
1,41210 |
1,40935 |
1,40629 |
||
48 |
1,41792 |
1,41627 |
1,41350 |
1,41042 |
||
50 |
1,42218 |
1,42051 |
1,41771 |
1,41462 |
||
52 |
1,42650 |
1,42480 |
1,42198 |
1,41888 |
||
54 |
1,43088 |
1,42917 |
1,42632 |
1,42321 |
||
56 |
1,43533 |
1,43360 |
1,43073 |
1,42761 |
||
58 |
1,43985 |
1,43809 |
1,43521 |
1,43208 |
||
60 |
1,44444 |
1,44266 |
1,43976 |
1,43661 |
||
62 |
1,44910 |
1,44730 |
1,44437 |
1,44122 |
||
64 |
1,45382 |
1,45201 |
1,44906 |
1,44590 |
||
66 |
1,45862 |
1,45679 |
1,45382 |
1,45066 |
||
68 |
1,46350 |
1,46164 |
1,45866 |
1,45549 |
||
70 |
1,46844 |
1,46657 |
1,46357 |
1,46039 |
||
72 |
1,47347 |
1,47157 |
1,46856 |
1,46537 |
||
74 |
1,47857 |
1,47665 |
1,47362 |
1,47044 |
||
76 |
1,48374 |
1,48181 |
1,47877 |
1,47558 |
||
78 |
1,48900 |
1,48705 |
1,48399 |
1,48080 |
||
80 |
1,49434 |
1,49237 |
1,48930 |
1,48610 |
||
82 |
1,49976 |
1,49777 |
1,49469 |
1,49149 |
||
84 |
1,50526 |
1,50326 |
1,50016 |
1,49697 |
||
| 6. Notes | ||||||
| 7. Reference | International Standard: ISO 1743 | |||||
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Keywords: laboratory method determination dry matter substance starch glucose maltose fructose syrup refraction refractive index