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International Starch Institute
Science Park Aarhus, Denmark
ISI 06 Table 2a - Determination of Dry Matter in Dual Converted 32 DE
Syrup by Refractive Index
| 1. Scope | The table is applicable to 32 DE dual converted syrup with 0.4% ash on dry matter. | LT 24 Nov. 1997 | ||||
| 2. Principle | The refractive index of sample is transformed to dry matter by a table. | |||||
| 3. Apparatus | 3.1 Refractometer with thermostat | |||||
| 4. Procedure | Adjust temperature of refractometer (3.1) to 20, 30, 45 or 60 oC. | +/- 0.2 oC | ||||
| Adjust sample temperature to that chosen for the refractometer. | ||||||
| Place a few drops of sample on fixed prism and close instrument | Work fast | |||||
| Read the refractive index (nD) to nearest 0.0002 unit. | Clean prisms immediately after. | |||||
| 5. Calculation | Find dry matter (DM) in percent of sample (average results of two samples with no decimal) by using table: | Correct eventually for differing DE | ||||
DM% |
20 oC |
30 oC |
45 oC |
60 oC |
||
0 |
1,33194 |
1,33194 |
1,32985 |
1,32725 |
||
2 |
1,33594 |
1,33487 |
1,33275 |
1,33012 |
||
4 |
1,33899 |
1,33788 |
1,33573 |
1,33308 |
||
6 |
1,34208 |
1,34095 |
1,33876 |
1,33608 |
||
8 |
1,34522 |
1,34406 |
1,34184 |
1,33914 |
||
10 |
1,34841 |
1,34723 |
1,34498 |
1,34225 |
||
12 |
1,35166 |
1,35045 |
1,34816 |
1,34541 |
||
14 |
1,35495 |
1,35372 |
1,35140 |
1,34863 |
||
16 |
1,35830 |
1,35704 |
1,35469 |
1,35190 |
||
18 |
1,36171 |
1,36042 |
1,35804 |
1,35522 |
||
20 |
1,36517 |
1,36385 |
1,36144 |
1,35860 |
||
22 |
1,36868 |
1,36734 |
1,36490 |
1,36204 |
||
24 |
1,37225 |
1,37088 |
1,36841 |
1,36554 |
||
26 |
1,37587 |
1,37448 |
1,37199 |
1,36909 |
||
28 |
1,37956 |
1,37814 |
1,37562 |
1,37270 |
||
30 |
1,38330 |
1,38186 |
1,37931 |
1,37637 |
||
32 |
1,38710 |
1,38564 |
1,38306 |
1,38010 |
||
34 |
1,39097 |
1,38948 |
1,38687 |
1,38390 |
||
36 |
1,39489 |
1,39338 |
1,39074 |
1,38775 |
||
38 |
1,39888 |
1,39734 |
1,39468 |
1,39167 |
||
40 |
1,40293 |
1,40137 |
1,39868 |
1,39566 |
||
42 |
1,40704 |
1,40546 |
1,40275 |
1,39971 |
||
44 |
1,41122 |
1,40962 |
1,40688 |
1,40383 |
||
46 |
1,41547 |
1,41384 |
1,41108 |
1,40801 |
||
48 |
1,41978 |
1,41813 |
1,41535 |
1,41227 |
||
50 |
1,42417 |
1,42249 |
1,41969 |
1,41659 |
||
52 |
1,42862 |
1,42692 |
1,42409 |
1,42098 |
||
54 |
1,43314 |
1,43142 |
1,42857 |
1,42545 |
||
56 |
1,43774 |
1,43600 |
1,43312 |
1,42999 |
||
58 |
1,44241 |
1,44065 |
1,43775 |
1,43461 |
||
60 |
1,44715 |
1,44537 |
1,44245 |
1,43930 |
||
62 |
1,45197 |
1,45017 |
1,44723 |
1,44407 |
||
64 |
1,45687 |
1,45504 |
1,45209 |
1,44892 |
||
66 |
1,46184 |
1,46000 |
1,45702 |
1,45385 |
||
68 |
1,46690 |
1,46503 |
1,46204 |
1,45886 |
||
70 |
1,47204 |
1,47015 |
1,46714 |
1,46395 |
||
72 |
1,47726 |
1,47535 |
1,47232 |
1,46913 |
||
74 |
1,48256 |
1,48064 |
1,47759 |
1,47439 |
||
76 |
1,48795 |
1,48601 |
1,48295 |
1,47974 |
||
78 |
1,49343 |
1,49147 |
1,48839 |
1,48518 |
||
80 |
1,49899 |
1,49701 |
1,49392 |
1,49071 |
||
82 |
1,50465 |
1,50265 |
1,49955 |
1,49633 |
||
84 |
1,51040 |
1,50839 |
1,50527 |
1,50205 |
||
| 6. Notes | ||||||
| 7. Reference | International Standard: ISO 1743 | |||||
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Keywords: laboratory method determination dry matter substance starch glucose maltose fructose syrup refraction refractive index