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International Starch Institute
Science Park Aarhus, Denmark
ISI 06 Table 2b - Determination of Dry Matter in Dual Converted 63 DE
Syrup by Refractive Index
| 1. Scope | The table is applicable to 63 DE dual converted syrup with 0.4% ash on dry matter. | LT 24 Nov. 1997 | ||||
| 2. Principle | The refractive index of sample is transformed to dry matter by a table. | |||||
| 3. Apparatus | 3.1 Refractometer with thermostat | |||||
| 4. Procedure | Adjust temperature of refractometer (3.1) to 20, 30, 45 or 60 oC. | +/- 0.2 oC | ||||
| Adjust sample temperature to that chosen for the refractometer. | ||||||
| Place a few drops of sample on fixed prism and close instrument | Work fast | |||||
| Read the refractive index (nD) to nearest 0.0002 unit. | Clean prisms immediately after. | |||||
| 5. Calculation | Find dry matter (DM) in percent of sample (average results of two samples with no decimal) by using table: | Correct eventually for differing DE | ||||
DM% |
20 oC |
30 oC |
45 oC |
60 oC |
||
0 |
1,33299 |
1,33194 |
1,32985 |
1,32725 |
||
2 |
1,33589 |
1,33481 |
1,33269 |
1,33006 |
||
4 |
1,33887 |
1,33777 |
1,33561 |
1,33296 |
||
6 |
1,34190 |
1,34077 |
1,33858 |
1,33590 |
||
8 |
1,34498 |
1,34382 |
1,34160 |
1,33890 |
||
10 |
1,34810 |
1,34691 |
1,34466 |
1,34194 |
||
12 |
1,35127 |
1,35006 |
1,34777 |
1,34503 |
||
14 |
1,35449 |
1,35325 |
1,35093 |
1,34816 |
||
16 |
1,35775 |
1,35649 |
1,35414 |
1,35135 |
||
18 |
1,36107 |
1,35978 |
1,35740 |
1,35459 |
||
20 |
1,36444 |
1,36312 |
1,36072 |
1,35788 |
||
22 |
1,36785 |
1,36651 |
1,36408 |
1,36122 |
||
24 |
1,37132 |
1,36996 |
1,36749 |
1,36462 |
||
26 |
1,37484 |
1,37345 |
1,37096 |
1,36807 |
||
28 |
1,37842 |
1,37700 |
1,37448 |
1,37157 |
||
30 |
1,38204 |
1,38061 |
1,37806 |
1,37513 |
||
32 |
1,38573 |
1,38426 |
1,38169 |
1,37874 |
||
34 |
1,38946 |
1,38798 |
1,38538 |
1,38241 |
||
36 |
1,39326 |
1,39175 |
1,38912 |
1,38614 |
||
38 |
1,39711 |
1,39557 |
1,39292 |
1,38992 |
||
40 |
1,40101 |
1,39946 |
1,39678 |
1,39376 |
||
42 |
1,40498 |
1,40340 |
1,40070 |
1,39767 |
||
44 |
1,40900 |
1,40740 |
1,40467 |
1,40163 |
||
46 |
1,41309 |
1,41146 |
1,40871 |
1,40565 |
||
48 |
1,41723 |
1,41558 |
1,41281 |
1,40974 |
||
50 |
1,42144 |
1,41977 |
1,41697 |
1,41389 |
||
52 |
1,42571 |
1,42402 |
1,42120 |
1,41810 |
||
54 |
1,43004 |
1,42833 |
1,42549 |
1,42238 |
||
56 |
1,43444 |
1,43271 |
1,42985 |
1,42673 |
||
58 |
1,43890 |
1,43715 |
1,43427 |
1,43114 |
||
60 |
1,44343 |
1,44166 |
1,43876 |
1,43562 |
||
62 |
1,44803 |
1,44624 |
1,44332 |
1,44017 |
||
64 |
1,45270 |
1,45088 |
1,44794 |
1,44479 |
||
66 |
1,45743 |
1,45560 |
1,45264 |
1,44948 |
||
68 |
1,46224 |
1,46039 |
1,45741 |
1,45425 |
||
70 |
1,46712 |
1,46525 |
1,46225 |
1,45908 |
||
72 |
1,47207 |
1,47018 |
1,46717 |
1,46400 |
||
74 |
1,47710 |
1,47519 |
1,47216 |
1,46898 |
||
76 |
1,48220 |
1,48027 |
1,47723 |
1,47405 |
||
78 |
1,48738 |
1,48543 |
1,48238 |
1,47919 |
||
80 |
1,49263 |
1,49067 |
1,48760 |
1,48442 |
||
82 |
1,49797 |
1,49599 |
1,49291 |
1,48972 |
||
84 |
1,50338 |
1,50139 |
1,49830 |
1,49511 |
||
| 6. Notes | ||||||
| 7. Reference | International Standard: ISO 1743 | |||||
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Keywords: laboratory method determination dry matter substance starch glucose maltose fructose syrup refraction refractive index