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International Starch Institute
Science Park Aarhus, Denmark
ISI 06 Table 2c - Determination of Dry Matter in Dual Converted 70 DE
Syrup by Refractive Index
| 1. Scope | The table is applicable to 70 DE dual converted syrup with 0.4% ash on dry matter. | LT 24 Nov. 1997 | ||||
| 2. Principle | The refractive index of sample is transformed to dry matter by a table. | |||||
| 3. Apparatus | 3.1 Refractometer with thermostat | |||||
| 4. Procedure | Adjust temperature of refractometer (3.1) to 20, 30, 45 or 60 oC. | +/- 0.2 oC | ||||
| Adjust sample temperature to that chosen for the refractometer. | ||||||
| Place a few drops of sample on fixed prism and close instrument | Work fast | |||||
| Read the refractive index (nD) to nearest 0.0002 unit. | Clean prisms immediately after. | |||||
| 5. Calculation | Find dry matter (DM) in percent of sample (average results of two samples with no decimal) by using table: | Correct eventually for differing DE | ||||
DM% |
20 oC |
30 oC |
45 oC |
60 oC |
||
0 |
1,33299 |
1,33194 |
1,32985 |
1,32725 |
||
2 |
1,33588 |
1,33480 |
1,33268 |
1,33005 |
||
4 |
1,33885 |
1,33774 |
1,33559 |
1,33293 |
||
6 |
1,34186 |
1,34073 |
1,33854 |
1,33587 |
||
8 |
1,34492 |
1,34377 |
1,34155 |
1,33884 |
||
10 |
1,34803 |
1,34685 |
1,34459 |
1,34187 |
||
12 |
1,35119 |
1,34997 |
1,34769 |
1,34494 |
||
14 |
1,35439 |
1,35315 |
1,35084 |
1,34807 |
||
16 |
1,35764 |
1,35638 |
1,35403 |
1,35124 |
||
18 |
1,36094 |
1,35965 |
1,35728 |
1,35446 |
||
20 |
1,36429 |
1,36297 |
1,36057 |
1,35773 |
||
22 |
1,36769 |
1,36635 |
1,36391 |
1,36106 |
||
24 |
1,37114 |
1,36977 |
1,36731 |
1,36444 |
||
26 |
1,37464 |
1,37325 |
1,37076 |
1,36786 |
||
28 |
1,37819 |
1,37678 |
1,37426 |
1,37135 |
||
30 |
1,38180 |
1,38036 |
1,37781 |
1,37488 |
||
32 |
1,38546 |
1,38399 |
1,38142 |
1,37847 |
||
34 |
1,38917 |
1,38768 |
1,38508 |
1,38212 |
||
36 |
1,39294 |
1,39143 |
1,38880 |
1,38582 |
||
38 |
1,39676 |
1,39523 |
1,39258 |
1,38958 |
||
40 |
1,40064 |
1,39909 |
1,39641 |
1,39339 |
||
42 |
1,40458 |
1,40300 |
1,40030 |
1,39727 |
||
44 |
1,40857 |
1,40697 |
1,40425 |
1,40120 |
||
46 |
1,41263 |
1,41100 |
1,40825 |
1,40520 |
||
48 |
1,41674 |
1,41509 |
1,41232 |
1,40925 |
||
50 |
1,42091 |
1,41924 |
1,41645 |
1,41337 |
||
52 |
1,42514 |
1,42345 |
1,42064 |
1,41754 |
||
54 |
1,42944 |
1,42773 |
1,42489 |
1,42179 |
||
56 |
1,43380 |
1,43207 |
1,42921 |
1,42609 |
||
58 |
1,43822 |
1,43647 |
1,43359 |
1,43046 |
||
60 |
1,44271 |
1,44093 |
1,43804 |
1,43490 |
||
62 |
1,44726 |
1,44547 |
1,44255 |
1,43941 |
||
64 |
1,45188 |
1,45007 |
1,44713 |
1,44398 |
||
66 |
1,45656 |
1,45473 |
1,45178 |
1,44862 |
||
68 |
1,46132 |
1,45947 |
1,45650 |
1,45334 |
||
70 |
1,46614 |
1,46427 |
1,46129 |
1,45812 |
||
72 |
1,47104 |
1,46915 |
1,46615 |
1,46298 |
||
74 |
1,47601 |
1,47410 |
1,47108 |
1,46791 |
||
76 |
1,48105 |
1,47912 |
1,47609 |
1,47291 |
||
78 |
1,48616 |
1,48422 |
1,48117 |
1,47799 |
||
80 |
1,49135 |
1,48939 |
1,48633 |
1,48315 |
||
82 |
1,49662 |
1,49464 |
1,49157 |
1,48839 |
||
84 |
1,50196 |
1,49997 |
1,49688 |
1,49370 |
||
| 6. Notes | ||||||
| 7. Reference | International Standard: ISO 1743 | |||||
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Keywords: laboratory method determination dry matter substance starch glucose maltose fructose syrup refraction refractive index