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International Starch Institute
Science Park Aarhus, Denmark
ISI 06 Table 3b - Determination of Dry Matter in Dual Converted
50 DE High Maltose Syrup by Refractive Index
| 1. Scope | The table is applicable to 50 DE dual converted high maltose syrup with 0.4% ash on dry matter. | LT 24 Nov. 1997 | ||||
| 2. Principle | The refractive index of sample is transformed to dry matter by a table. | |||||
| 3. Apparatus | 3.1 Refractometer with thermostat | |||||
| 4. Procedure | Adjust temperature of refractometer (3.1) to 20, 30, 45 or 60 oC. | +/- 0.2 oC | ||||
| Adjust sample temperature to that chosen for the refractometer. | ||||||
| Place a few drops of sample on fixed prism and close instrument | Work fast | |||||
| Read the refractive index (nD) to nearest 0.0002 unit. | Clean prisms immediately after. | |||||
| 5. Calculation | Find dry matter (DM) in percent of sample (average results of two samples with no decimal) by using table: | Correct eventually for differing DE | ||||
DM% |
20 oC |
30 oC |
45 oC |
60 oC |
||
0 |
1,33299 |
1,33194 |
1,32985 |
1,32725 |
||
2 |
1,33592 |
1,33484 |
1,33272 |
1,33009 |
||
4 |
1,33894 |
1,33783 |
1,33568 |
1,33302 |
||
6 |
1,34200 |
1,34087 |
1,33868 |
1,33600 |
||
8 |
1,34511 |
1,34395 |
1,34173 |
1,33903 |
||
10 |
1,34827 |
1,34708 |
1,34483 |
1,34211 |
||
12 |
1,35148 |
1,35027 |
1,34798 |
1,34523 |
||
14 |
1,35474 |
1,35350 |
1,35118 |
1,34841 |
||
16 |
1,35805 |
1,35678 |
1,35444 |
1,35164 |
||
18 |
1,36141 |
1,36012 |
1,35774 |
1,35492 |
||
20 |
1,36482 |
1,36350 |
1,36110 |
1,35826 |
||
22 |
1,36828 |
1,36694 |
1,36451 |
1,36165 |
||
24 |
1,37180 |
1,37044 |
1,36797 |
1,36509 |
||
26 |
1,37538 |
1,37399 |
1,37149 |
1,36859 |
||
28 |
1,37901 |
1,37759 |
1,37507 |
1,37215 |
||
30 |
1,38269 |
1,38125 |
1,37870 |
1,37576 |
||
32 |
1,38643 |
1,38497 |
1,38239 |
1,37944 |
||
34 |
1,39023 |
1,38874 |
1,38614 |
1,38317 |
||
36 |
1,39409 |
1,39257 |
1,38994 |
1,38696 |
||
38 |
1,39800 |
1,39647 |
1,39381 |
1,39081 |
||
40 |
1,40198 |
1,40042 |
1,39774 |
1,39472 |
||
42 |
1,40602 |
1,40444 |
1,40173 |
1,39869 |
||
44 |
1,41012 |
1,40851 |
1,40578 |
1,40273 |
||
46 |
1,41428 |
1,41265 |
1,40990 |
1,40683 |
||
48 |
1,41851 |
1,41686 |
1,41408 |
1,41100 |
||
50 |
1,42280 |
1,42113 |
1,41832 |
1,41523 |
||
52 |
1,42716 |
1,42546 |
1,42264 |
1,41953 |
||
54 |
1,43158 |
1,42986 |
1,42702 |
1,42390 |
||
56 |
1,43607 |
1,43434 |
1,43147 |
1,42834 |
||
58 |
1,44064 |
1,43888 |
1,43599 |
1,43285 |
||
60 |
1,44527 |
1,44349 |
1,44058 |
1,43743 |
||
62 |
1,44997 |
1,44817 |
1,44524 |
1,44209 |
||
64 |
1,45475 |
1,45293 |
1,44998 |
1,44682 |
||
66 |
1,45960 |
1,45776 |
1,45479 |
1,45162 |
||
68 |
1,46452 |
1,46266 |
1,45968 |
1,45650 |
||
70 |
1,46953 |
1,46765 |
1,46465 |
1,46146 |
||
72 |
1,47461 |
1,47271 |
1,46969 |
1,46650 |
||
74 |
1,47977 |
1,47785 |
1,47481 |
1,47162 |
||
76 |
1,48501 |
1,48307 |
1,48002 |
1,47682 |
||
78 |
1,49033 |
1,48837 |
1,48531 |
1,48211 |
||
80 |
1,49573 |
1,49376 |
1,49068 |
1,48748 |
||
82 |
1,50122 |
1,49923 |
1,49614 |
1,49294 |
||
84 |
1,50680 |
1,50479 |
1,50169 |
1,49848 |
||
| 6. Notes | ||||||
| 7. Reference | International Standard: ISO 1743 | |||||
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Keywords: laboratory method determination dry matter substance starch glucose maltose fructose syrup refraction refractive index